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, C Hunter, and G L Jones, J Chromatography, 192, 228 (1980) Sullivan, A B, J Org Chem, 31, 2811 (1966) Sundet, S A, Macromolecules, 11, 146 (1978) Takagi, T, J Appl Polym Sci, 19, 1649 (1975) Takayanagi, M and T Katayose, J Polym Sci Polym Chem Ed, 21, 31 (1983) Taylor, R T, Polymer-Bound Oxidizing Agents, Chap 7 in Polymeric Reagents and Catalysts, W T Ford, ed, Am Chem Soc Symp Ser, Vol 308, American Chemical Society, Washington, D C, 1986 Tazuke, S and H Kimura, J Polym Sci Polym Lett Ed, 15, 93 (1977); Makromol Chem, 179, 2603 (1978) Tomoi, M and W T Ford, Polymeric Phase Transfer Catalysts, Chap 5 in Synthesis and Separations Using Functional Polymers, D C Sherrington and P Hodge, eds, Wiley, New York, 1988 Toy, P H and K D.

Janda, Acc Chem Res, 33, 546 (2000) Tran, A and J Prud homme, Macromolecules, 10, 149 (1977) Tundo, P, Synthesis, 315 (1978) Turbak, A, Rayon, pp 45 72 in Encyclopedia of Polymer Science and Engineering, 2nd ed, Vol 14, H F Mark, N M Bikales, C G Overberger, and G Menges, eds, Wiley-Interscience, New York, 1988 Van Boom, J H, Heterocyclics, 7, 1197 (1977) Vogl, O, Pure Appl Chem, 51, 2409 (1979) Vogl, O and D Tirrell, J Macromol Sci Chem, A13, 415 (1979) Vogl, O, A C Albertsson, and Z Janovic, Polymer, 26, 1288 (1985) Vukov, R, Rubber Chem Technol, 57, 275 (1984) Waller, F J, Catalysis with a Per uorinated Ion-Exchange Polymer, Chap 3 in Polymeric Reagents and Catalysts, W T Ford, ed, Am Chem Soc Symp Ser, Vol.

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As noted above, between 1964 and 1971, the Treasury issued no longterm bonds Annual issues commenced in 1971, but the outstanding stock of marketable government bonds actually continued to decline through 1974, as more bonds matured than were issued and the Treasury relied increasingly on shorter-term bills and notes to finance its then-modest deficits That trend changed in 1975, when the outstanding stock of marketable long-term governments began to increase Between 1974 and 1989, as the national debt soared, the marketable proportion consisting of bonds increased from one-eighth to one-sixth, an absolute rise from $33 billion to over $300 billion The table on the next two pages lists the chief long-term issues of 1971 1989, a few of which were exchange offerings without a cash price.

308, American Chemical Society, Washington, D C, 1986 Walz, R and W Heitz, J Polym Sci Polym Chem Ed, 16, 1807 (1978)..

Ward, W. J. and T. J. McCarthy, Surface Modi cation, pp. 674 689 in Encyclopedia of Polymer Science and Engineering, 2nd ed. (supplement), H. F. Mark, N. M. Bikales, C. G. Overberger, and G. Menges, eds., Wiley-Interscience, New York, 1989. Wilson, J. E., Radiation Chemistry of Monomers, Polymers, and Plastics, Chap. 7, Marcel Dekker, New York, 1974. Wingard, L. B., Jr., E. Katchalski-Katzir, and L. Goldstein, eds., Enzyme Technology, Vol. 2 in Applied Biochemistry and Bioengineering, Academic Press, New York, 1979. Wolfe, J. R., Jr., T. L. Pugh, and A. S. Killian, Rubber Chem. Technol., 41, 1329 (1968). Wrana, C., K. Reinartz, H. R. Winkelbach, Macromol. Mater. Eng., 286, 657 (2001). Wulff, G., I. Schulze, and K. Zabrocki, Makromol. Chem., 181, 531 (1980). Yamamoto, K., Y. Miwa, H. Tanaka, M. Sakaguchi, and S. Shimada, J. Polym. Sci. Polym. Chem. Ed., 40, 3350 (2002). Yamazaki, T. and T. Seguchi, J. Polym. Sci. Polym. Chem. Ed., 38, 3383 (2000). Yaroslavsky, C., A. Patchornik, and E. Katchalski, Tetrahedron Lett., 3629 (1970). Yoshida, J., I. J. Hashimoto and N. Kawabata, Bull. Chem. Soc. Jpn., 54, 309 (1981). Yu, Y. and G. R. Brown, Macromolecules, 27, 7121, 7127 (1994). Zhang, L.-M., Macromol. Mater. Eng., 286, 267 (2001). Zhao, B. and W. J. Brittain, Macromolecules, 33, 8813 (2000).

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PROBLEMS 9-1 What reactions can be used to crosslink the following polymers a. Polyester from ethylene glycol and maleic anhydride b. Polyester from ethylene glycol, phthalic acid, and oleic acid c. cis-1,4-Polyisoprene d. Polydimethylsiloxane e. Polyethylene f. Cellulose g. Chlorosulfonated polyethylene Describe the crosslinking reactions by equations. Show by equations the synthesis of each of the following: a. Cellulose acetate b. Cellulose nitrate c. Methyl cellulose d. Poly(vinyl formal) Show by equations each of the following: a. Chlorination of polyethylene b. Chlorination of 1,4-polyisoprene c. Chlorosulfonation of polyethylene d. Synthesis of an anionic ion-exchange polymer from polystyrene e. Cyclization of 1,4-polyisoprene by HBr Show the structure of each of the following: a. Poly(propene-b-styrene) b. Poly(styrene-g-methyl methacrylate)

Because of the frequency of the Treasury s trips to the bond market in these two decades, the progression of coupon rates and average new issue yields provides a fairly accurate portrayal of the dramatic moves of the long-term market in these years Interest rates, both long and short, declined moderately during 1976, the year of lowest inflation since 1972 The following year, 1977, was one of contrasts Prime corporate bond yields were remarkably stable from month to month; they touched a low of 792% in September, which was to prove the low point of the corporate market between early 1974 and the 1990 s, and averaged only 23 basis points higher in December than in January Long-term governments rose somewhat more over the course of the year, narrowing the spread between corporates and governments.

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